![]() Any ideas or code examples i could look into? I tried to compare the load sequence of game.exe and the only difference i noticed that it seems to find this data section within d2data.mpq, while for me it doesn't, maybe i didn't initialize something correctly yet. In advance i already loaded the mpq files by calling win.dll#10059. It seems to fail on loading "data\\local\\font\\LATIN\\default.map". Lang.dll#1033 (which initializes the language tables) in 1.12 crashes. If the mixture is very polar, the pre-adsorbtion procedure is preferable as the use of too much EtOAc will compromise the resolution.I figured it out and i am now loading D2Client.dll instead which loads storm.dll, the problem i have now is that i am unable to initialize the language. If necessary a small amount of EtOAc can be added to dissolve more polar compounds. 11įor small columns (< 4 cm) it is usually easier to dissolve the mixture in a small volume of n-heptane and add it evenly onto the surface of the column with a pipette. 40 g on a column with a diameter of 10 cm) and still achieve good separation of mixtures with a ΔR f ≅ 0.05 (by analytical TLC). In general we have found that it is possible to load a mixture of up to approx. All chromatography should be performed in a hood behind a safety shield. Special care should be taken when using a separatory funnel as it is not designed for this purpose. The inventors of Flash Column Chromatography stressed on the fact that Flash Column Chromatography is pressure- and not vacuum driven.Īlthough we have never experienced any problems, it is important to use precaution with evacuated glassware. Liquid chromatography - purification - large scale chromatography Virtual Golden Anniversary Issue – 50 Years Synthesis.20 most-cited SYNTHESIS articles published in 2020/2021.Golden Anniversary Issue – 50 Years Synthesis – Part I.Golden Anniversary Issue – 50 Years Synthesis – Part II.Amination Reactions in Organic Synthesis.Halogenation Methods (with a View Towards Radioimaging Applications).Domino C–H Functionalization/Cascade Catalysis.Recent Advances in Amide Bond Formation.Recent Advances in Metal-Catalyzed Ring Construction.Special Issue Dedicated to Professor Shinji Murai – Part I.Special Issue Dedicated to Professor Shinji Murai – Part II.Cycloadditions – Established and Novel Trends – in Celebration of the 70th Anniversary of the Nobel Prize Awarded to Otto Diels and Kurt Alder.Bürgenstock Special Section 2021 – Future Stars in Organic Chemistry.SYNTHESIS Conference Special Topic ISyS圜at21. ![]()
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